What you will need to build your bucket can be
purchased at the yellowish orange store.
WHAT YOU WILL NEED
Heat resistant Epoxy (paint
area)
7.5 Litre Polypropylene Bucket with
ruber "O" ring in lids seal (paint aisle, the bucket can be can be
smaller)
Scrap Plexi Glass (far back, to the
right)
Plexi-glass cutter (ask
someone)
Shank washer (plumbing isle)
Fan ( buy a fan, two would be
better)
Get the Shank washer you
purchased.
Stare at it.
Now get the lid for your
bucket.
Simply drill a hole in the center of
the lid using a 7/8th's drill bit.
Place the washer flush over the hole
and use your Epoxy to create a bond/seal between the two.
Now you will want to create a window or
two or three then add the plexi-glass. Carefully carve out your
windows.
I cut out three to give it some
personality. It hasn't spoken yet..
If you think you can make do without
the windows, go for yours. It's funta$tic to
know whats going on during the rxn.
Make SURE you use HEAT RESISTANT epoxy.
1.5L of MeOH
800mg of HgCl2
55g of Heavy Duty Al.
Ketone (mdp2p) and
Nitromethane
50ml's
____________________________40ml's
Rig.
On the very top you will see an
addition funel, then a claisen, then the column, then the condensor.
Fans blowing on the column and the
bucket.
1.4L of water was combined with 524g of
NaOH, then allowed to cool.
This was added to the Rxn contents, in
the same bucket
Stir
.
Post Rxn contents
Next, 1L of toluene was added to the
mix.
Stir
At this point your fairly happy at the
cleanliness of this process.
Everything is done in the same bucket,
and stirring has never been easier!
Here comes the hardest part if the
whole process.
You will need to pour as much toluene
off the top as you can without spilling any.
At this point you can find your own
creative way to get the freebase out and into your sep
funnel..
I tilted the bucket back and used a
500ml measuring cup to gather the top freebase layer.
After collecting the freebase,
another 750ml of toluene was added, stirred, and
collected..
1.75L of toluene freebase.
l
Washed 1.75L of freebase with 2L of
saturated NaCl
Washed again with 2L of saturated
baking soda.
Washed 2x with 2L of clean
water.
Dried with 80g of Anhydrous Epsoms
salts.
Dwarfer style gas rig
MDMA hcl. forming in the non polar
solution.
You should have close to 40g of mdma
hcl.
The best part about this process is the
ability to cook a larger batch without having to use an overhead
stirrer.
Cook done using 2x scale of MM's
beautiful write up.
4x scale would cut it close when it
comes time to basify and extract, but its definetly possible.
That's next on the list!
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