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FA | RX(1); FLST(1); RX(3) |
Reaction (1 of 1)
Reaction ID | 1767866 |
Reactant BRN | 136380 |
Reactant | 5-allyl-benzo[1,3]dioxole |
Product BRN | 156510 |
Product | 3-benzo[1,3]dioxol-5-yl-propionaldehyde |
No. of Reaction Details | 3 |
Reaction Details (1 of 1)
Reaction Classification | Preparation |
Reagent | 1.) disiamylborane; 2.) PCC |
Other Conditions | 1.) ether, 2 h, 0 deg C; 2.) CH2Cl2, reflux, 2 h |
Comment | Yield given. Multistep reaction |
Citation Pointer | 5620640; Journal; Brown, Herbert C.; Kulkarni, Surendra U.; Rao, C. Gundu; Patil, Vemanna D.; TETRAB; Tetrahedron; EN; 42; 20; 1986; 5515-5522; |
Reaction Details (2 of 1)
Reaction Classification | Preparation |
Reagent | 1.) Sia2BH, 2.) pyridinium chlorochromate |
Other Conditions | 1.) ether, 0 deg C, 2.) CH2Cl2, reflux |
Comment | Yield given. Multistep reaction |
Citation Pointer | 5573006; Journal; Brown, Herbert C.; Kulkarni, Surendra U.; Rao, C. Gundu; SYNTBF; Synthesis; EN; 2; 1980; 151-153; |
Reaction Details (3 of 1)
Reaction Classification | Multistage |
Yield | 81 percent (BRN=156510) |
No. of Stages | 2 |
Stage 1 | |
Stage 2 | |
Reagent | acetoxyborohydride; pyridinium chlorochromate |
Solvent | tetrahydrofuran; CH2Cl2 |
Time | 16 hour(s); 1 hour(s) |
Temperature | 20 |
Other Conditions | Heating |
Citation Pointer | 6324491; Journal; Dhillon, Ranjit S.; Kaur, Avinder Pal; Kaur, Gurpreet; JICSAH; J.Indian Chem.Soc.; EN; 77; 9; 2000; 453 - 454; |
Reference (1 of 3)
Citation Number | 5573006 |
Document Type | Journal |
Authors | Brown, Herbert C.; Kulkarni, Surendra U.; Rao, C. Gundu |
CODEN | SYNTBF |
Journal Title | Synthesis |
Language Code | EN |
Number | 2 |
Publication Year | 1980 |
Page | 151-153 |
Reference (2 of 3)
Citation Number | 5620640 |
Document Type | Journal |
Authors | Brown, Herbert C.; Kulkarni, Surendra U.; Rao, C. Gundu; Patil, Vemanna D. |
CODEN | TETRAB |
Journal Title | Tetrahedron |
Language Code | EN |
(Series) Volume | 42 |
Number | 20 |
Publication Year | 1986 |
Page | 5515-5522 |
Reference (3 of 3)
Citation Number | 6324491 |
Document Type | Journal |
Authors | Dhillon, Ranjit S.; Kaur, Avinder Pal; Kaur, Gurpreet |
CODEN | JICSAH |
Journal Title | J.Indian Chem.Soc. |
Language Code | EN |
(Series) Volume | 77 |
Number | 9 |
Publication Year | 2000 |
Page | 453 - 454 |